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http://yadda.icm.edu.pl:80/baztech/element/bwmeta1.element.baztech-article-BUJ5-0005-0039

Czasopismo

Polish Journal of Chemistry

Tytuł artykułu

Synthesis, Characterization and Electrochemical Property of Dicyclohexyl-18-crown-6 Nickel(II) Bis(dithiolate) Complexes

Autorzy Sun, Y.  Dong, F.  Dou, J.  Li, D.  Gao, X.  Wang, D. 
Treść / Zawartość
Warianty tytułu
Języki publikacji EN
Abstrakty
EN Two organic-inorganic hybrid dicyclohexyl-18-crown-6 nickel(II) bis(dithiolate) complexes, [K(DC18C6-B)]2[Ni(mnt)2] (1) and [K(DC18C6-A)]2[Ni(i-mnt)2] (2) (DC18C6-A = cis-syn-cis-dicyclohexyl-18-crown-6; DC18C6-B = cis-anti-cis-dicyclohexyl- 18-crown-6; mnt = maleonitriledithiolate; i-mnt = isomaleonitriledithiolate), have been synthesized by the reactions of dicyclohexyl-18-crown-6with NiCl2 andK2(mnt) or K2(i-mnt) respectively, and characterized by elemental analysis, FT-IR,UV-Vis spectroscopy and X-ray single crystal diffraction. They both crystallize triclinic, space group P1. Complex 1 shows a neutral molecule composed of two [K(DC18C6-B)]+ complex cations and one [Ni(mnt)2]2– complex anion via two K–N coordination bonds. In complex 2, the [K(DC18C6-A)]+ complex cation and [Ni(i-mnt)2]2– complex anion afford a 1D chain- like structure by N–K–N interactions.
Słowa kluczowe
EN dicyclohexyl-18-crown-6   nickel bis(dithiolate) complex   synthesis and crystal structure  
Wydawca Polskie Towarzystwo Chemiczne
Czasopismo Polish Journal of Chemistry
Rocznik 2006
Tom Vol. 80, nr 12
Strony 2001--2009
Opis fizyczny Bibliogr. 36 poz., rys.
Twórcy
autor Sun, Y.
autor Dong, F.
autor Dou, J.
autor Li, D.
autor Gao, X.
autor Wang, D.
  • Department of Chemistry, Liaocheng University, Liaocheng, 252059, P. R. China
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