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http://yadda.icm.edu.pl:80/baztech/element/bwmeta1.element.baztech-article-BUJ5-0005-0036

Czasopismo

Polish Journal of Chemistry

Tytuł artykułu

Coordination Chemistry of Nickel(II), Copper(II), and Cobalt(II) with MN4 Core-Containing Two Novel vic-Dioximes Ligands. Synthesis, Spectroscopy and Redox Properties

Autorzy Kilic, A.  Tas, E.  Gumgum, B.  Yilmaz, I. 
Treść / Zawartość
Warianty tytułu
Języki publikacji EN
Abstrakty
EN Two new vic-dioxime, N-(4-amino-1-benzyl piperidine)-anti-phenylglyoxime (L1H2) and N-(4-amino-1-benzyl piperidine)-anti-glyoxime (L2H2) were prepared by the reaction of anti-phenylchloroglyoxime and anti-monochloroglyoxime with 4-amino- 1-benzyl piperidine in absolute THF at –15°C. Mononuclear nickel(II), copper(II), and cobalt(II) complexes have a metal-ligand ratio of 1:2 in which the ligands coordinate through the two nitrogen atoms as do most vic-dioximes. The ligands and their Co(II), Cu(II), and Ni(II) complexes were characterized by elemental analyses, FT-IR, UV-vis, 1H-NMR and 13C-NMR, magnetic susceptibility measurements, electrical conductivity measurements and cyclic voltammetry. The electrical conductivity of Ni(II), Co(II), and Cu(II) metal complexes were measured using Four-Point Probe analysis. The electrochemical behavior of theNi(II), Co(II), andCu(II) complexeswere investigated by cyclic voltammetry in DMSO.
Słowa kluczowe
EN vic-dioxime   metal complexes   synthesis   redox properties   molar conductivity  
Wydawca Polskie Towarzystwo Chemiczne
Czasopismo Polish Journal of Chemistry
Rocznik 2006
Tom Vol. 80, nr 12
Strony 1967--1981
Opis fizyczny Bibliogr. 48 poz., rys.
Twórcy
autor Kilic, A.
autor Tas, E.
autor Gumgum, B.
autor Yilmaz, I.
  • Department of Chemistry, Harran University, Sanliurfa 63510, Turkey
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