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Performance of a new HPLC chiral stationary phase derived from N-(3,5-dinitrobenzoyl)-D-α-phenylglycine with a quinoxaline branching unit

Identyfikatory
Warianty tytułu
Języki publikacji
EN
Abstrakty
EN
A new brush-type HPLC chiral stationary phase (CSP) comprising π-acidic N-(3,5-dinitrobenzoyl)-D-α-phenylglycine chiral units bound to the quinoxaline units of modified γ-aminopropyl silica gel by a 1,2-diaminoethane spacer has been prepared by solid-phase synthesis. To test the CSP attempts were made to separate the enantiomers of twenty-two racemates with different functional groups and the results were compared with those obtained by use of three structurally related chiral stationary phases.
Słowa kluczowe
EN
Rocznik
Tom
Strony
97--107
Opis fizyczny
Bibliogr. 16 poz., rys., tab.
Twórcy
autor
autor
  • Laboratory for Stereoselective Catalysis and Biocatalysis, Rudjer Boskovic Institute, P.O. Box 180, Bijenicka cesta 54, HR-10002 Zagreb, Croatia
Bibliografia
  • [1] J. Kern and K. Kirkland in L.R. Snyder, J.J. Kirkland, and J.L. Glajch (Eds) Practical HPLC Method Development, J. Wiley and Sons, New York, 1997, pp. 537–615
  • [2] H.Y. Aboul-Enein and I. Ali, Chiral Separations by Liquid Chromatography and Related Technologies, Marcel Dekker, New York, 2003
  • [3] (a) W.H. Pirkle and T.C. Pochapsky, Chem Rev., 89, 347 (1989); (b) D.R. Taylor and K. Maher, J. Chromatogr. Sci., 30, 67 (1992)
  • [4] (a) M.H. Hyun and C.-S. Min, Bull. Kor. Chem. Soc., 17, 1117 (1996); (b) M.H. Hyun, M.S. Na, and C.-S. Min, J. Chromatogr. A, 732, 209 (1996)
  • [5] C.J. Welch, J. Chromatogr. A, 666, 3 (1994)
  • [6] L. Oliveros, C. Minguillón, B. Desmaiéres, and P.-L. Desbéne, J. Chromatogr., 589, 53 (1992)
  • [7] M.H. Hyun, Y.D. Kim, S.C. Han, and J.B. Lee, J. High Resol. Chromatogr., 21, 464 (1998)
  • [8] W.H. Pirkle, D.W. House, and J.M. Finn, J. Chromatogr., 192, 143 (1980)
  • [9] N. Oi, H. Kitahara, F. Aoki, and N. Kisu, J. Chromatogr. A, 689, 195 (1995)
  • [10] D. Kontrec, A. Abatangelo, V. Vinković, and V. Šunjić, Chirality, 13, 294 (2001)
  • [11] B. Zafirova, G. Landek, D. Kontrec, V. Šunjić, and V. Vinković, Croat. Chem. Acta, 77, 573 (2004)
  • [12] M.H. Hyung, C.-S. Min, and K.K. Jyung, Bull. Korean Chem. Soc., 17, 409 (1996)
  • [13] C.A. Obafemi and W. Pfleiderer, Molecules, 9, 223 (2004)
  • [14] R. Kaliszan, M.P. Marszall, M.J. Markuszewski, T. Bączek, and J. Pernak, J. Chromatogr. A, 1030, 263 (2004)
  • [15] B. Buszewski, M. Jezierska, M. Welniak, and D. Berek, J. High Resol. Chromatogr., 21, 267 (1998)
  • [16] S.C. Dhanesar in S. Ahuja (Ed) Chiral Separations by Liquid Chromatography, American Chemical Society, Washington DC, 1991, pp. 183–202
Typ dokumentu
Bibliografia
Identyfikator YADDA
bwmeta1.element.baztech-article-BAT8-0006-0042
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