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Polish Journal of Chemical Technology

Tytuł artykułu

Comparison of photoacoustic, diffuse reflectance, attenuated total reflectance and transmission infrared spectroscopy for the study of biochars

Autorzy Pasieczna-Patkowska, S.  Madej, J. 
Treść / Zawartość
Warianty tytułu
Języki publikacji EN
EN Four infrared spectroscopic techniques - photoacoustic (PAS), diffuse reflectance (DRS), attenuated total reflectance (ATR) and transmission (TS) - were evaluated for the qualitative analysis of the biochar obtained from willow feedstock during pyrolysis. Increase in pyrolysis temperature resulted in more aromatic and carbonaceous structure of biochars. These changes could easily be detected from Fourier transform infrared (FT-IR) spectral differences. The comparison of the spectra obtained by the four FT-IR techniques allowed to conclude that there are differences in the spectra acquired using different IR technique caused by different signal acquisition. PAS and ATR were the best techniques used in order to obtain spectra with smooth and sharp peaks, in contrast to TS, where bands were less-separated. DRS turned out to be the weakest of all techniques, due to poor spectral quality and poor separation of the bands.
Słowa kluczowe
EN biochar   surface analysis   infrared spectroscopy  
Wydawca West Pomeranian University of Technology. Publishing House
Czasopismo Polish Journal of Chemical Technology
Rocznik 2018
Tom Vol. 20, nr 4
Strony 75--83
Opis fizyczny Bibliogr. 39 poz., rys., tab.
autor Pasieczna-Patkowska, S.
autor Madej, J.
  • Lublin University of Technology, Department of Geotechnics, Faculty of Civil Engineering and Architecture, 40 Nadbystrzycka Str., 20-618 Lublin, Poland
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Opracowanie rekordu w ramach umowy 509/P-DUN/2018 ze środków MNiSW przeznaczonych na działalność upowszechniającą naukę (2019).
Kolekcja BazTech
Identyfikator YADDA bwmeta1.element.baztech-a8c41a6a-3c36-49c9-8ff0-1cf4be29bbc7
DOI 10.2478/pjct-2018-0057