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http://yadda.icm.edu.pl:80/baztech/element/bwmeta1.element.baztech-73068d47-10a1-4b5b-85a0-2246959fbc81

Czasopismo

Advances in Materials Science

Tytuł artykułu

Cr/Fe Ratio by Xps Spectra of Magnetoelectropolished Aisi 316L SS Using Linear, Shirley and Tougaard Methods of Background Subtraction

Autorzy Hryniewicz, T.  Rokosz, K. 
Treść / Zawartość http://content.sciendo.com/view/journals/adms/adms-overview.xml
Warianty tytułu
Języki publikacji EN
Abstrakty
EN In the paper, the analyses of Fe2p3/2 and chromium Cr2p3/2 XPS spectra with fitting by symmetrical and asymmetrical line shapes as well as using Linear, Shirley and Tougaard Method of Background Subtraction are presented. The calculations are performed on AISI 316L SS biomaterial after magnetoelectropolishing MEP operation. It was found, the chromium-to-iron ratio after magnetoelectropolishing MEP for other analyses could be in the range from 2.2 to 6.2 depending on the line shapes as well as type of backgrounds used to XPS spectra fitting. The most important for comparison the surface layers concerning the Cr/Fe ratio is to use the same line shape and backgrounds for all analyses.
Słowa kluczowe
EN XPS spectra fitting   linear   Shirley   Tougaard Backgrounds   316L SS   Magnetoelectropolishing MEP   Cr/Fe ratio  
Wydawca Politechnika Gdańska
Czasopismo Advances in Materials Science
Rocznik 2013
Tom Vol. 13, nr 1(35)
Strony 11--20
Opis fizyczny Bibliogr. 16 poz., rys., tab
Twórcy
autor Hryniewicz, T.
  • Koszalin University of Technology, Division of Surface Electrochemistry and Engineering, Faculty of Mechanical Engineering, Racławicka 15-17, 75-620 Koszalin, Poland, Tadeusz.Hryniewicz@tu.koszalin.pl
autor Rokosz, K.
  • Koszalin University of Technology, Division of Surface Electrochemistry and Engineering, Faculty of Mechanical Engineering, Racławicka 15-17, 75-620 Koszalin, Poland, rokosz@tu.koszalin.pl
Bibliografia
1. Rokosz K., Polerowanie elektrochemiczne stali w polu magnetycznym (Electrochemical polishing of steels in the magnetic field), Monograph Nr 219, Publisher: Koszalin University of Technology, Koszalin 2012, ISSN 0239-7129, (211 pages, in Polish).
2. Hryniewicz T., Rokicki R., Rokosz K., Magnetoelectropolishing for metal surface modification, Transactions of the Institute of Metal Finishing, 2007, 85(6), 325-332.
3. Hryniewicz T., Concept of microsmoothing in electropolishing process, Surfaceand Coatings Technology, 1994, 64(2), 75-80.
4. Hryniewicz T., Rokosz K., Polarization Characteristics of Magnetoelectropolishing Stainless Steels, Materials Chemistry and Physics, 2010, 122, 169-174.
5. Simka W., Mosiałek M., Nawrat G., Nowak P., Żak J., Szade J., Winiarski A., Maciej A., Szyk-Warszyńska L., Electrochemical polishing of Ti-13Nb-13Zr Alloy, Surface and Coatings Technology, 2012, 213, 239-246.
6. Hryniewicz T., Rokicki R., Rokosz K., Surface characterization of AISI 316L biomaterials obtained by electropolishing in a magnetic field, Surface & Coatings Technology, 2008, 202(9), 1668-1673.
7. Hryniewicz T., Rokosz K., Rokicki R., Electrochemical and XPS Studies of AISI 316L Stainless Steel after Electropolishing in a Magnetic Field, Corrosion Science, 2008, 50(9), 2676-2681.
8. Hryniewicz T., Rokicki R., Rokosz K., Corrosion Characteristics of Medical Grade AISI 316L Stainless Steel Surface after Electropolishing in a Magnetic Field, CORROSION (The Journal of Science and Engineering), Corrosion Science Section, 2008, 64(8), 660-665.
9. Rokicki R., US Patent No 7632390, http://www.patentgenius.com/patent/7632390.html
10. Product Data Bulletin, 316/316L Stainless Steel, AK Steel Corporation, PD-140 7180-0127 PDF 7/00, 2000; www.aksteel.com
11. Hryniewicz T., Rokosz K., Investigation of selected surface properties of AISI 316L SS after magnetoelectropolishing, Materials Chemistry and Physics, 2010, 123, 47-55; DOI: 10.1016/j.matchemphys.2010.03.060
12. Fairley N., http://www.casaxps.com, © Casa software Ltd., 2005,
13. Walton J., Carrick A., The Casa Cookbook-The CasaXPS User’s Manual, Part 1: Recipes for XPS data proceedings, 2009, ISBN: 9780954953300, Publisher: Acolyte Science.
14. CasaXPS Processing Software, CasaXPS Manual 2.3.15 Rev 1.0, Copyright © 2010 Casa Software Ltd, 19-20.
15. Herrera-Gomez A., The Peak-Shirley Background (Shirley background in overlapping peaks), Centro de Investigación y de Estudios Avanzados del IPN Unidad Querétaro, Internal Report Created 8/2011, Last Update 2/2012, (14 pages).
16. Biesinger M.C., Payne B.P., Grosvenor A. P., Lau L. W. M., Gerson A. R., Smart R. St. C., Resolving surface chemical states in XPS analysis of first row transmission metals, oxides and hydroxides: Cr, Mn, Fe, Co and Ni, Applied Surface Science, 2011, 257, 2717-2730.
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