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http://yadda.icm.edu.pl:80/baztech/element/bwmeta1.element.baztech-550ea51d-7ce6-4a0a-8356-a829513c5ef7

Czasopismo

Advances in Materials Science

Tytuł artykułu

Xps Study Of Aisi 316L Ss Surfaces After Mechanical And Electrochemical Polishing and Chelating/Electro-Chelating Treatments

Autorzy Rokosz, K.  Hryniewicz, T. 
Treść / Zawartość http://content.sciendo.com/view/journals/adms/adms-overview.xml
Warianty tytułu
Języki publikacji EN
Abstrakty
EN In the paper, there are presented the analyses of iron Fe2p3/2and chromium Cr2p3/2and oxide O1s XPS spectra of surfaces obtained after abrasive and electrochemical polishing with additional treatment as chemical chelating in the solution containing of 10% Citric Acid and 2% Ethylenediaminetetraacetic Acid. There was also performed electro-chelating after mechanical polishing in the electrolyte for chemical chelating. The maximum values of chromium compounds to iron compounds ratio were obtained after electropolishing with and without stirring with chemical chelating in Citric Acid and EDTA and they were in rage from 3.5 to 3.6. The minimum value was obtained for the steel surface after abrasive polishing and electro-chelating and was equal 1.3. After electrochemical polishing and chemical passivation in the surface layer there were detected FeO and Cr(OH)3as dominated compounds. After abrasive polishing and electro-chelating there were mostly Fe2O3and Cr2O3.
Słowa kluczowe
EN XPS spectra fitting   Surface layer   AISI 316L SS   Electropolishing   Chelating   Passivation   Electrochelating   Cr/Fe ratio   Fe 2p   Cr 2p   O 1s  
Wydawca Politechnika Gdańska
Czasopismo Advances in Materials Science
Rocznik 2014
Tom Vol. 14, nr 1(39)
Strony 31--41
Opis fizyczny Bibliogr. 18 poz., rys., tab.
Twórcy
autor Rokosz, K.
  • Koszalin University of Technology, Faculty of Mechanical Engineering, Racławicka 15-17 75-620 Koszalin, Poland, rokosz@tu.koszalin.pl
autor Hryniewicz, T.
  • Koszalin University of Technology, Faculty of Mechanical Engineering, Racławicka 15-17 75-620 Koszalin, Poland
Bibliografia
1. Rokosz K., Electrochemical polishing of steels in magnetic field, Monograph No. 219, Publisher: Koszalin University of Technology, Koszalin 2012, ISSN 0239-7129, (in Polish).
2. Hryniewicz T., Rokicki R., Rokosz K., Magnetoelectropolishing for metal surface modification, Transactions of the Institute of Metal Finishing, 2007, 85(6), 325-332.
3. Hryniewicz T., Rokicki R., Rokosz K., Surface characterization of AISI 316L biomaterials obtained by electropolishing in a magnetic field, Surface & Coatings Technology, 2008, 202(9 1668-1673. ), 1-16.
4. Hryniewicz T., Rokosz K., Rokicki R., Electrochemical and XPS Studies of AISI 316L Stainless Steel after Electropolishing in a Magnetic Field, Corrosion Science, 2008, 50(9), 2676-2681.
5. Hryniewicz T., Rokicki R., Rokosz K., Corrosion Characteristics of Medical Grade AISI 316L Stainless Steel Surface after Electropolishing in a Magnetic Field, Corrosion, 2008, 64(8), 660-665.
6. Rokicki R., US Patent No. 7632390, http://www.patentgenius.com/patent/7632390.html
7. Davidson J.A. , Kovacs P., Passivation method and passivated implant, 1992, Patent EP 0520721 A2.
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10. Cleaning, Derouging and Passivation of the Stainless Steel Parts of the Purified Water Systems in Standard Operating Procedure, www.gmpsop.com, 1-10.
11. Cleaning and passivating of stainless steel equipment, Applications/Cleaning Procedures C-1.30, Technical Reference, Ecolab, 2010, 1-6.
12. Wegrelius L., Sjödén B., Passivation treatment of stainless steel, Acom, Outokumpu, 2004 , 2-9
13. Fairley N., http://www.casaxps.com, © Casa software Ltd. 2005.
14. Walton J., Carrick A., The Casa Cookbook-The CasaXPS User’s Manual, Part 1: Recipes for XPS data processings, 2009, ISBN: 9780954953300, Publisher: Acolyte Science.
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16. Herrera-Gomez A., The Peak-Shirley Background (Shirley background in overlapping peaks), Centro de Investigación y de Estudios Avanzados del IPN Unidad Querétaro, Internal Report Created 8/2011, Last Update 2/2012, 14 pages.
17. Biesinger M.C., Payne B.P., Grosvenor A.P., Lau L.W.M., Gerson A.R., Smart R.St.C., Resolving surface chemical states in XPS analysis of first row transition metals, oxides and hydroxides: Cr, Mn, Fe, Co and Ni, Applied Surface Science, 2011, 257, 2717-2730.
18. Rokosz K., Hryniewicz T., Cr/Fe Ratio by XPS Spectra of Magnetoelectropolished AISI 316L SS using Linear, Shirley and Tougaard Method of Background Subtraction, Advances in Materials Science 13(1) (2013) 11-20; DOI: 10.2478/adms-2013-0002
Kolekcja BazTech
Identyfikator YADDA bwmeta1.element.baztech-550ea51d-7ce6-4a0a-8356-a829513c5ef7
Identyfikatory
DOI 10.2478/adms‐2014‐0004